超清版 GB/T 44428-2024 化妆品中大麻二酚和四氢大麻酚的测定 液相色谱-串联质谱法

ICS 71.100.70
CCS Y 42
中华人民共和国国家标准
GB/T 44428—2024
化妆品中大麻二酚和四氢大麻酚的测定
液相色谱﹘串联质谱法
Determination of cannabidiol and tetrahydrocannabinol in cosmetics—
Liquid chromatography tandem mass spectrometry
2024-08-23 发布2025-03-01 实施
国家市场监督管理总局
国家标准化管理委员会发 布

目　　次
前言 ····································································································· Ⅲ
引言 ····································································································· Ⅳ
1 范围 ·································································································· 1
2 规范性引用文件 ······················································································ 1
3 术语和定义 ··························································································· 1
4 原理 ·································································································· 1
5 试剂和材料 ··························································································· 1
6 仪器设备 ······························································································ 2
7 试样制备和试验步骤 ················································································· 2
7.1 试样制备 ························································································· 2
7.2 测定参考条件 ···················································································· 2
7.3 定性测定 ························································································· 3
7.4 定量测定 ························································································· 3
7.5 空白试验 ························································································· 4
8 试验数据处理 ························································································· 4
9 回收率 ································································································ 4
10 精密度 ······························································································· 4
附录A （资料性） 标准品的信息 ······································································ 5
附录B （资料性） 标准溶液多反应监测色谱图 ······················································· 6
附录C （资料性） 方法回收率偏差范围 ······························································ 7
参考文献 ·································································································· 8


前　　言
本文件按照 GB/T 1.1—2020《标准化工作导则　第1 部分：标准化文件的结构和起草规则》的规
定起草。
请注意本文件的某些内容可能涉及专利。本文件的发布机构不承担识别专利的责任。
本文件由中国轻工业联合会提出。
本文件由全国香料香精化妆品标准化技术委员会（SAC/TC 257）归口。
本文件起草单位：上海市质量监督检验技术研究院、上海市食品药品检验研究院、上海海关动植物
与食品检验检疫技术中心、上海香料研究所有限公司、清华大学。
本文件主要起草人： 薛峰、杨晋青、印杰、郑荣、陈丹丹、牛云蔚、陈章庭、杨斌、陈瑶、
喻怡静、彭兴盛、石玲玲、杨振宇、顾宇翔、王怡、张岩、王正。

引　　言
本文件的被测物质是我国《化妆品安全技术规范（2015 年版）》规定的禁用原料。
禁用原料是指不得作为化妆品原料使用的物质。《化妆品安全技术规范（2015 年版）》规定：